Synthesis, Growth and Material Characterization of Bis L-Alanine Triethanol Amine (BLATEA) Single Crystals Grown by Slow Evaporation Technique

Studies on the Growth and Characterization of N- methyl-4-nitroaniline Organic Single Crystal Grown by Slow Evaporation Technique

An organic material N-methyl-4-nitroaniline (NMNA) has been grown by the slow evaporation technique at ambient temperature. The grown NMNA crystal crystallized using three different solvents such as tetrahydrofuran (THF), dimethylsulfoxide (DMSO) and acetone, respectively. The grown crystal system and crystallinity were determined by single crystal and powder X-ray diffraction (XRD) analysis. F...

synthesis and characterization of some macrocyclic schiff bases

ماکروسیکلهای شیف باز از اهمیت زیادی در شیمی آلی و دارویی برخوردار می باشند. این ماکروسیکلها با دارابودن گروه های مناسب در مکانهای مناسب می توانند فلزاتی مثل مس، نیکل و ... را در حفره های خود به دام انداخته، کمپلکسهای پایدار تولید نمایند. در این پایان نامه ابتدا یک دی آلدئید آروماتیک از گلیسیرین تهیه می شود و در مرحله بعدی واکنش با دی آمینهای آروماتیک و یا آلیفاتیک در رقتهای بسیار زیاد منجر به ت...

Synthesis, Growth and Characterization of Nonlinear Optical Bis(2-aminopyridinium) Sulfate Single Crystals

Synthesis and Characterization of Cadmium Sulfide Crystals Grown by DVT Technique

Cadmium Sulfide crystals were grown by direct vapor transport (DVT) from high-purity starting materials. The grown CdS crystals were orange in color, transparent, dendrite platelets shaped were observed. The structure of CdS crystals has been studied with the help of X-ray diffraction (XRD) and Transmission Electron Microscope (TEM). The crystals grown by DVT technique possess hexagonal structu...

GROWTH OF ZnS SINGLE CRYSTALS BY CVT TECHNIQUE UNDER DIFFERENT MASS TRANSPORT STABILITY CONDITIONS

Abstract: A thermodynamic model was used to find out the optimum temperature for the growth of ZnS single crystals in closed ampoules by chemical vapor transport technique. Based on this model 1002 °C was found to be optimum temperature for 2 mg/cm3 concentration of transporting agent (iodine). ZnS Crystals were grown in optimum (1002 °C) and non-optimum (902 °C and 1102 °C) temperatures. The c...